This data publication contains the raw, derived, and processed data related to investigations into solid tablet dosage form production using drop-on-demand dispensing of active pharmacetuical ingredients. UV-Vis spectroscopy, THz Raman spectroscopy, and mass spectrometry chemical data for pharmaceutical-grade excipients, warfarin sodium, doxycycline, citalopram HBr, levothyroxine, fluoxetine, oxycodone, and acetaminophen are provided. SEM and high speed visualization, and drop counting print log data are included. Processed data from linear least squares calibration, uncertainty, and various parametric analyses (personalized dose production, taper regimen production, dissolution studies, content uniformity measurments, etc) are provided in tabulated data files.*Any mention of commercial products is for information only; it does not imply recommendation or endorsement by NIST.