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Field portable X-ray fluorescence and associated quality-control data for paint chips sampled from selected sites in Lakeport, Lake County, California

Metadata Updated: July 6, 2024

This data -release component documents field portable X-ray fluorescence (pXRF) measurements of lead and associated quality-control data for 19 samples of paint chips collected from structures suspected to have legacy coatings of lead-based paint in Lakeport (Lake County, California) during July 11-12, 2022. Environmental samples were collected at selected sites to assess the effects of lead-based paint on soil chemistry. This sampling was made as part of a broader study to attribute sources of lead in soils in cooperation with the California Department of Toxic Substances Control (DTSC) for their Lead-Acid Battery Recycling Facility Investigation and Cleanup (LABRIC) program. Lead concentrations for paint chips measured by pXRF were used as a semi-quantitative screening tool to aid in selection of sites for soil and paint-chip sampling in addition to the age of structure and condition of exterior paint layers. A total of 34 measurements of lead concentration using pXRF for 19 samples of paint chips are included in this child item. Measurements were made on layered paint chips contained within low-density, polyethylene sample bags using a Thermo Niton XL5 pXRF instrument. Layered paint chip samples were scanned through both their inner and outer facing sides to assess relative lead contents of newer and older paint layers. Measurements on multiple paint chips from the same sample bag are presented for two samples. Field and laboratory measurements of standard reference materials with lead concentrations within the range of values measured for paint-chip samples had percent recoveries for lead concentration within 20 percent of the certified value. The same standard reference materials were measured in the laboratory inside 2 millimeter-thickness, low-density polyethylene sample bags and had percent recoveries for lead concentration within 20 percent of the certified value. Lead concentrations for paint chips analyzed by pXRF presented in this data release are reported in parts per million and rounded to one to two significant figures to provide conservative, order-of-magnitude estimates of apparent paint-chip lead concentrations. Apparent lead concentrations for layered paint chips are not representative of the concentration of paint in an individual paint layer, as the density and thickness of different paint layers with different elemental compositions can influence pXRF results (McKnight and others, 1989). This data release contains two tab-delimited text files. The "Lakeport_paint.txt" file contains field pXRF measurements of lead for paint-chip samples. The "Lakeport_pXRF_QC.txt" file contains quality control data for pXRF measurements of lead for four National Institute of Standards and Technology (NIST)-certified standard reference materials.

Access & Use Information

Public: This dataset is intended for public access and use. License: No license information was provided. If this work was prepared by an officer or employee of the United States government as part of that person's official duties it is considered a U.S. Government Work.

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Dates

Metadata Created Date July 19, 2023
Metadata Updated Date July 6, 2024

Metadata Source

Harvested from DOI EDI

Additional Metadata

Resource Type Dataset
Metadata Created Date July 19, 2023
Metadata Updated Date July 6, 2024
Publisher U.S. Geological Survey
Maintainer
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Identifier USGS:649075c5d34ef77fcb002fe5
Data Last Modified 20230817
Category geospatial
Public Access Level public
Bureau Code 010:12
Metadata Context https://project-open-data.cio.gov/v1.1/schema/catalog.jsonld
Metadata Catalog ID https://datainventory.doi.gov/data.json
Schema Version https://project-open-data.cio.gov/v1.1/schema
Catalog Describedby https://project-open-data.cio.gov/v1.1/schema/catalog.json
Harvest Object Id 2abdcbe3-9a20-4d26-93fe-62bfbdbac53c
Harvest Source Id 52bfcc16-6e15-478f-809a-b1bc76f1aeda
Harvest Source Title DOI EDI
Metadata Type geospatial
Old Spatial -122.95,39.01,-122.88,39.07
Publisher Hierarchy White House > U.S. Department of the Interior > U.S. Geological Survey
Source Datajson Identifier True
Source Hash 2d4e4a9592e03d91bfd092812c9aee881be0d4a91793b98ba9a365fbfcc7fa0c
Source Schema Version 1.1
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