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    • Dataset for Overcoming Analytical Challenges of Other Test Method 50: Analysis of Volatile Fluorinated Compounds in Passivated Canisters from Stationary Source Emissions

    Metadata Updated: August 18, 2025

    This dataset includes spreadsheets containing raw data that were used to create the figures and tables in the publication. Target responses, retention times, and calculations associated with mass spectrometry analyses of Other Test Method 50 canister standards and samples are included. These data were used to construct calibration curves and to calculate percent recoveries and biases of target compounds in the presence of high carbon dioxide (CO2) levels. The dataset also include calculations of average concentrations, standard deviations, relative standard deviations, and percent recoveries for replicate injections to calculate method detection limits (MDLs) and to evaluate percent increases and in sample concentrations by analyzing samples using different thermal desorption method parameters. The data also include an evaluation of method precision, including averages, relative standard deviations, and percent differences between canister samples collected in the absence and presence of high CO2 levels.

    This dataset is associated with the following publication: Wallace, A., S. Jackson, B. Preston, L. Miles, H. Calder, S. Davies, and M. Cumbes. Overcoming analytical challenges of Other Test Method 50: Analysis of volatile fluorinated compounds in passivated canisters from stationary source emissions. JOURNAL OF CHROMATOGRAPHY A. Elsevier Science Ltd, New York, NY, USA, 1759: 1, (2025).

    Access & Use Information

    Public: This dataset is intended for public access and use. License: See this page for license information.

    Downloads & Resources

    References

    https://doi.org/10.1016/j.chroma.2025.466226

    Dates

    Metadata Created Date August 18, 2025
    Metadata Updated Date August 18, 2025

    Metadata Source

    Harvested from EPA ScienceHub

    Other Data Resources

    Additional Metadata

    Resource Type Dataset
    Metadata Created Date August 18, 2025
    Metadata Updated Date August 18, 2025
    Publisher U.S. EPA Office of Research and Development (ORD)
    Maintainer
    Identifier https://doi.org/10.23719/1531889
    Data Last Modified 2025-07-31
    Public Access Level public
    Bureau Code 020:00
    Schema Version https://project-open-data.cio.gov/v1.1/schema
    Harvest Object Id 98405611-a1fe-44b4-9df8-8243eb9e6894
    Harvest Source Id 04b59eaf-ae53-4066-93db-80f2ed0df446
    Harvest Source Title EPA ScienceHub
    License https://pasteur.epa.gov/license/sciencehub-license.html
    Program Code 020:000
    Publisher Hierarchy U.S. Government > U.S. Environmental Protection Agency > U.S. EPA Office of Research and Development (ORD)
    Related Documents https://doi.org/10.1016/j.chroma.2025.466226
    Source Datajson Identifier True
    Source Hash db763ecd9dbf0d849576c758bf14321a3e92ca7a941058b107938aa0db31b0b5
    Source Schema Version 1.1

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