Chemical and isotopic composition of gas, water, and solids from the 2019-2020 water lake in Halema’uma’u Crater, Kīlauea Volcano, Hawaii: Chemical composition of solids filtered from water samples
Samples of the crater lake water were filtered in the field with a 0.45 micron filter. Subsequently, additional precipitates formed in the solute-rich samples (secondary precipitates). The solids that accumulated on the filters (both secondary and original precipitate) were digested by heating overnight in a sealed Teflon vial with 300 µL concentrated HCl, 100 µL concentrated HNO3, and 500 µL concentrated HF. Following digestion, samples were dried down, then re-dissolved in 300 µL concentrated HNO3 and diluted with MilliQ water. The liquid from the digested samples were analyzed for element concentrations by inductively coupled plasma-optical emission spectrometry (ICP-OES) using a ThermoFisher ICAP 6500 Duo at the U.S. Geological Survey laboratories in Menlo Park, California.
Find Related Datasets
Search by Tags
Click any tag below to search for similar datasets
Complete Metadata
| @type | dcat:Dataset |
|---|---|
| accessLevel | public |
| bureauCode |
[
"010:12"
]
|
| contactPoint |
{
"fn": "Sara E Peek",
"@type": "vcard:Contact",
"hasEmail": "mailto:speek@usgs.gov"
}
|
| description | Samples of the crater lake water were filtered in the field with a 0.45 micron filter. Subsequently, additional precipitates formed in the solute-rich samples (secondary precipitates). The solids that accumulated on the filters (both secondary and original precipitate) were digested by heating overnight in a sealed Teflon vial with 300 µL concentrated HCl, 100 µL concentrated HNO3, and 500 µL concentrated HF. Following digestion, samples were dried down, then re-dissolved in 300 µL concentrated HNO3 and diluted with MilliQ water. The liquid from the digested samples were analyzed for element concentrations by inductively coupled plasma-optical emission spectrometry (ICP-OES) using a ThermoFisher ICAP 6500 Duo at the U.S. Geological Survey laboratories in Menlo Park, California. |
| distribution |
[
{
"@type": "dcat:Distribution",
"title": "Digital Data",
"format": "XML",
"accessURL": "https://doi.org/10.5066/P99H412X",
"mediaType": "application/http",
"description": "Landing page for access to the data"
},
{
"@type": "dcat:Distribution",
"title": "Original Metadata",
"format": "XML",
"mediaType": "text/xml",
"description": "The metadata original format",
"downloadURL": "https://data.usgs.gov/datacatalog/metadata/USGS.61d371b4d34ed79293fe6e31.xml"
}
]
|
| identifier | http://datainventory.doi.gov/id/dataset/USGS_61d371b4d34ed79293fe6e31 |
| keyword |
[
"Hawai'i",
"Kilauea",
"USGS:61d371b4d34ed79293fe6e31",
"elemental analysis",
"geoscientificInformation",
"sulfur isotopes"
]
|
| modified | 2023-03-30T00:00:00Z |
| publisher |
{
"name": "U.S. Geological Survey",
"@type": "org:Organization"
}
|
| spatial | -155.29700, 19.39400, -155.26400, 19.42000 |
| theme |
[
"geospatial"
]
|
| title | Chemical and isotopic composition of gas, water, and solids from the 2019-2020 water lake in Halema’uma’u Crater, Kīlauea Volcano, Hawaii: Chemical composition of solids filtered from water samples |
