This data set documents results of analysis of samples collected from the Arctic National Wildlife Refuge during Summer 2019. Data tables include: 1. The numeric and alphanumeric identifiers for samples collected for this study and the dates these samples were collected; 2. Results data containing concentration values of individual polycyclic aromatic hydrocarbon compounds in sediment, soil, and vegetation samples; 3. Results data containing concentration values of individual PAH compounds in water samples; 4. Results data containing concentration values of individual polycyclic aromatic hydrocarbon compounds in quality-control sample blanks for all four sample matrices (sediment, soil, vegetation, water); 5. Results data containing mass values of individual polycyclic aromatic hydrocarbon compounds detected in quality-control procedural spiked and purified water spiked samples that were spiked with mixture of polycyclic aromatic hydrocarbon compounds; 6. Results data containing concentration values of individual polycyclic aromatic hydrocarbon compounds in sediment, soil, and vegetation samples subsampled in triplicate; 7. Results data containing percent recovery values of deuterated polycyclic aromatic hydrocarbon surrogate compounds spiked into all processed samples at the beginning of the sample preparation procedure as a measure to determine recovery of targeted polycyclic aromatic hydrocarbon compounds subjected to the sample preparation procedure